High Temperature Real-Time X-Ray Diffraction Analysis
Real-time high temperature x-ray diffraction (XRD) is a powerful analytical technique used to study phase transformations in materials as they are subjected to varying temperatures. Unlike traditional XRD methods, which only capture data at a single temperature point, real-time high-temperature XRD enables continuous monitoring of material phase changes throughout heating and cooling processes. This approach provides critical insights into how materials such as ceramics, metals, and oxides behave under extreme thermal conditions, making it essential for industries like aerospace, energy, and advanced materials research. By identifying phase transitions in real-time, this method helps optimize material properties, predict performance, and accelerate development cycles.

Our high-temperature XRD analysis is particularly valuable in industries that require precision in materials development, including advanced ceramics, metals, and oxides. Whether you're in research and development or production, real-time insights into phase transitions can significantly enhance your material performance and reduce costly experimental runs.
The challenge of phase transformation monitoring
Predicting and monitoring phase changes at elevated temperatures is a critical, yet challenging, aspect of materials science. Traditional methods often require multiple tests to capture the full range of transformations a material may undergo, leading to resource-intensive processes. Novel and complex materials, particularly those designed for high-temperature applications, can behave unpredictably when subjected to thermal cycles, complicating the development and testing process.
Lucideon’s High Temperature Real-Time XRD Analysis provides a robust solution to these challenges by enabling multiple, real-time measurements. This allows for a deeper understanding of phase changes during heating or cooling, streamlining the R&D process.
Lucideon's real-time high temperature XRD offering
Our service is designed to deliver precise, real-time data on phase transitions, offering the following benefits:
- Dynamic phase monitoring: multiple XRD scans at varying temperatures allow for continuous observation of material phase changes, enabling detailed analysis of when and how transformations occur. This is especially useful when the temperature of phase transition is unknown or when stability assessments are required
- Phase prediction and validation: our high-temperature XRD service not only confirms predicted phases but also identifies novel or unexpected phases that may emerge during the heating process, such as distorted calcium-rich phases
- Efficient experimentation: by reducing the number of experimental runs needed, Lucideon’s real-time XRD accelerates material development, delivering faster, more reliable results. This method is ideal for projects that require detailed understanding of phase behavior during synthesis or operation
Key benefits
- Enhanced material insights: gain a comprehensive understanding of how material phases evolve under real-world conditions, improving material selection and optimizing performance for high-temperature applications
- Cost and time efficiency: our approach minimizes the need for repeated experimental runs while maximizing data output, significantly reducing both time and costs associated with material development
- Accelerated research and development: with the ability to quickly screen and analyse novel oxide materials, metals, and ceramics, our service supports faster innovation and material refinement
Applications
- Materials development and research: our XRD analysis is ideal for researchers and developers working on advanced materials, particularly for high-temperature applications in industries such as aerospace, energy, and automotive.
- Synthesis projects: perfect for projects where the behavior of materials during heating needs detailed exploration or where phase transformations are not well understood.
- Operational monitoring: monitor phase changes in materials under real-world operating conditions to predict performance and improve material durability and reliability.
Why choose Lucideon?
Lucideon combines state-of-the-art technology with expert knowledge to deliver unparalleled insights into high-temperature phase transformations. Our real-time high temperature XRD analysis service provides detailed, actionable data that can help reduce the cost and time associated with material testing and development. Whether you’re working with complex oxide systems or exploring new high-temperature materials, our XRD services offer the precision and reliability needed to drive successful outcomes.
Contact us to discover how we can help.